某铁矿强磁尾矿反浮选回收试验研究

针对我国西部某铁矿强磁选尾矿进行了反浮选回收铁资源的试验研究, 探讨了pH值、抑制剂可溶性淀粉用量、阳离子捕收剂十二胺用量对浮选指标的影响。结果表明, 在矿浆pH=10、可溶性淀粉用量2 400 g/t、十二胺用量400 g/t条件下进行一粗一精(精选药剂用量减半)闭路反浮选, 可获得铁品位43.88%、回收率50.93%的铁精矿产品。     

粗金粉中金的氯浸-控制电位还原精炼

某冶炼厂氰化金泥还原得到的粗金产品纯度较低，采用氯浸-还原工艺对粗金进行了精炼提纯。在生产工艺中采用盐酸+氯酸钠对粗金进行氯浸溶解，用焦亚硫酸钠控制电位选择性还原浸出液中的金。采用补水-冷却使银和铅从氯浸液充分沉淀析出，通过调整pH值、改变焦亚硫酸钠添加方式、精确控制还原电位等方法，产品金锭达到IC-Au99.99标准。两年的生产实践创造了明显的经济效益。     

Performance of Holstein and Swedish-Red × Jersey/Holstein crossbred dairy cows within low- and medium-concentrate grassland-based systems

This 2 × 2 factorial design experiment was conducted to compare the performance of spring-calving Holstein dairy cows (HOL, n = 34) with Swedish Red × Jersey/Holstein crossbred (SR × J/HOL, n = 34) dairy cows within low and medium concentrate input grassland-based dairy systems. The experiment commenced when cows calved and encompassed 1 full lactation. Cows were offered diets containing grass silage and concentrates [70:30 dry matter (DM) ratio, and 40:60 DM ratio, for low and medium, respectively] until turnout, grazed grass plus either 1.0 or 4.0 kg of concentrate/d during the grazing period (low and medium, respectively), and grass silage and concentrates (85:15 DM ratio, and 70:30 DM ratio, for low and medium, respectively) from rehousing and until drying off. No significant genotype × system interactions were present for any of the feed intake or full-lactation milk production data examined. Full-lactation concentrate DM intakes were 769 and 1,902 kg/cow for the low and medium systems, respectively, whereas HOL cows had a higher total DM intake than SR × J/HOL cows in early lactation, but not in late lactation. Although HOL cows had a higher lactation milk yield than SR × J/HOL cows, the latter produced milk with a higher fat and protein content, and thus fat plus protein yield was unaffected by genotype. Milk produced by the SR × J/HOL cows had a higher degree of saturation of fatty acids than milk produced by the HOL cows, and the somatic cell score of milk produced by the former was also higher. Throughout the lactation, HOL cows were on average 30 kg heavier than SR × J/HOL cows, whereas the SR × J/HOL cows had a higher body condition score than the HOL cows. Holstein cows had a higher incidence of mastitis and ovarian dysfunction that SR × J/HOL cows.     

铂钯精矿中氯化银的浸出预处理研究

铜阳极泥分铜液所得铂钯精矿中的银主要以氯化银(AgCl)形态存在，可用氨水或亚硫酸钠作为浸出剂去除银。绘制了Ag⁺与NH3、SO2- 3配体组分图，结合电位-pH图分析表明，氨浸的pH值范围为7.7~13.5，亚硫酸钠浸出宜在中性或碱性条件下进行。优化条件实验结果表明，银的氨浸浸出率为95.3%，碲浸出率为14.9%，有微量铂、钯浸出；以亚硫酸钠为浸出剂，银的浸出率为97.3%，碲浸出率为11.5%，金、铂和钯均不被浸出。亚硫酸钠更适于作为铂钯精矿预处理除银的浸出剂。     

Simultaneous extraction of gold and zinc from refractory carbonaceous gold ore by chlorination roasting process

A novel process based on chlorination roasting was proposed to simultaneously recover gold and zinc from refractory carbonaceous gold ore by using NaCl as chlorination agent. The effects of roasting temperature, roasting time and NaCl content on the volatilization rates of gold and zinc were investigated. The reaction mechanism and the phase transition process were also analyzed by means of SEM, EDS and XRD. The results demonstrated that under the optimal conditions of NaCl content of 10%, roasting temperature of 800 °C, roasting time of 4 h and gas flow rate of 1 L/min, the rates of gold and zinc were 92% and 92.56%, respectively. During low-temperature chlorination roasting stage, a certain content of sulfur was beneficial to the chlorination reactions of gold and zinc; and during high-temperature chlorination roasting stage, the crystal structure of vanadium-bearing mica was destroyed, and the vanadium-containing oxides were beneficial to the chlorinating volatilization of gold and zinc. Eventually, the chlorinated volatiles of gold and zinc could be recovered by alkaline solution.     

某高硫难处理金精矿超细磨提金试验研究

针对某高硫难处理金精矿中金大部分被黄铁矿包裹、直接氰化浸出金浸出率低的问题,采用超细磨-碱预处理-氰化浸出工艺处理金精矿,通过条件优化可获得金浸出率84.50%,氰化钠耗量控制在3 kg/t以内,该工艺简单、流程短、安全环保。     

硫酸装置转化换热器泄漏维修的实践

介绍了新洋丰农业科技股份有限公司200 kt/a硫精砂制酸装置转化工序工艺流程及存在的问题。经过分析查找,由于转化工序Ⅲ换热器和Ⅳa换热器存在泄漏,导致转化率偏低。临时停车后采用烟饼初步测出换热器泄漏的大致位置和面积,再采用压缩空气逐根换热管打压试漏,精准找出泄漏的换热管,进行堵头两侧封堵维修,维修后总转化率由99.33%提高到99.60%,氨法尾气脱硫系统氨耗大幅下降,质量分数20%氨水的消耗量由10 t/d下降到3 t/d。     

我国典型黄金矿业上市公司财务报表比较分析

避险属性决定了黄金价格走势与全球经济基本面息息相关,进而影响黄金矿业公司财务数据。为及时掌握黄金价格震荡下跌背景下我国黄金矿业行业发展情况,本文以我国黄金矿业行业的3家上市公司为例,对其2012~2018年财务年报进行了统计计算,对比研究了3家黄金公司的偿债能力、盈利能力和营运能力,进而结合杜邦模型,综合分析了3家黄金上市公司的财务和经营状况。结果表明：紫金矿业盈利能力较强,而山东黄金资产使用效率较好,中金黄金在盈利能力和资产使用效率方面相对还需全面提升,结合近年来黄金矿业公司生产运营中典型共性问题的总结分析,给出了相应的财务管理改进建议,可为同类矿业公司的财务分析和优化调整提供参考。     

Superabsorbent dewatering of refractory gold concentrate slurries

In this paper, superabsorbent polymer (SAB) dewatering behaviour of selected mineral pulps comprising low-grade, refractory gold flotation concentrate, bio-oxidation product and cyanide leach residue was investigated as an alternative to conventional, gravity thickening. The shear rheology of the resulting sediments was also investigated for pulp handleability. All slurries displayed better SAB-mediated dewatering performance, in terms of reduced processing time, volume minimization and greater water recovery for recycle, in comparison with gravity thickening. Specifically, SAB absorbed >94 wt.% water from the dilute slurries within 30 min of contact time. 45–76 wt.% more water was recovered after 60 min at high supernatant clarity using the SAB dewatering approach compared with gravity settling. The observed non-Newtonian, shear thinning rheological behaviour of SAB-dewatered consolidated slurries, reflecting low to moderate yield stresses in the range 1–40 Pa and shear thinning viscosities (<10 mPa⋅s), indicate their “handleability” in hydro-transport. The cost effectiveness of the SAB dewatering process engendered by its significantly greater water recovery and SAB polymer recovery, regeneration and multiple reuse capacity.     

大洋多金属硫化物冶炼性能研究

主要针对我国多金属硫化物勘探合同区样品产出的精矿开展冶炼工艺方案研究，考察其冶金性能，综合回收其有价金属。通过试验研究，富锌多金属硫化物精矿经焙烧-酸浸后，锌和铜浸出率可分别达到99.22%和96.71%，贵金属主要富集于浸出渣中，为我国大洋多金属硫化物的冶金技术开发提供依据。